C4.4 Engines for Caterpillar Built Machines Caterpillar


Diesel Exhaust Fluid Quality - Test

Usage:

AP500F 449

Required Tooling

Table 1
Required Tools 
Tool  Part Number  Part Description  Qty 
431-7087  Refractometer (DEF) 
162-5791  Towel 
169-8373  Fluid Sampling Bottle 
1U-5718  Vacuum Pump 
4C-4600  Container 
1U-7648  Tube Cutter 
466-8796  Test Strip 
1U-8757  Tube  Length as needed 
457-6144  Tool As - Pliers 

Test Procedure

DEF Removal Procedure

Note: For Diesel Exhaust Fluid (DEF) handling and storage procedures, refer to Operation and Maintenance Manual, Fluid Recommendations for more information.

  1. Clean the DEF tank of all debris prior to removal of any component. Contamination of the DEF can affect results of testing.


    Illustration 1g03706721
    Typical example
    (1) DEF tank fill cap
    (2) Filter screen

  2. Remove fill cap (1) from the Diesel Exhaust Fluid (DEF) tank.

  3. Use Tooling (J) to press and release the tabs. With the tabs released, remove the filter screen (2) from DEF tank neck adapter.


    Illustration 2g03706724
    Typical example
    (3) Vacuum pump nut
    (4) Tooling (D)
    ( 5) Tooling (H)

    Note: To ensure that the DEF sample is not contaminated during extraction, use a new piece of Tooling (H) every time this procedure is performed.

  4. Remove Tooling (H) from the plastic bag and install into Tooling (D).

    1. Loosen nut (3) to install Tooling (H).

    2. Install Tooling (H) all the way through the cap of the vacuum pump as shown in Illustration 2.

    3. Tighten the nut on top of the vacuum pump down completely to prevent DEF leaks.

  5. Remove Tooling (C) from the plastic bag. Remove the cap and install Tooling (C) onto Tooling (D).


    Illustration 3g03706727
    Typical example
    (5) Tooling (H)
    ( 6) DEF tank filler neck

    Note: The DEF sample must only be taken from the top level of fluid that is contained in the DEF tank. The top level of the DEF is where the contaminants will be located.

  6. Place the other end of Tooling (H) into the filler neck of DEF tank (6).

  7. Extract DEF from the top level of fluid in the tank using Tooling (D). Fill Tooling (C) to the "Fill Line" that is on the bottle.

  8. Proceed to"Test Procedure For DEF Contamination" to begin contamination testing.

Test Procedure For DEF Contamination

  1. Place Tooling (G) into Tooling (C) for 5 seconds.

    Note: The test strips should be able to detect for the presence of hydrocarbons.



    Illustration 4g03707382
    (7) Negative test result
    (8) Positive test result

  2. Remove Tooling (G) and look for discoloring as shown in Illustration 4. Any discoloring of Tooling (G) indicates DEF contamination by an oil-based fluid. Contact the Dealer Solution Network (DSN) for further information.

    Note: If the test strips indicate no DEF contamination, proceed to step 3.

    Note: Clean water should be used to wash spilled DEF off machine components and surfaces.

    Note: Wear gloves when handling the DEF filter.



    Illustration 5g06278274
    (1) Protective cover

  3. Remove protective cover (1).


    Illustration 6g06278289
    (2) DEF filter cap

  4. Use a suitable tool to remove DEF filter cap (2).

    Remove protective cover (1).



    Illustration 7g06278325
    (3) Compensator

  5. With the filter installed in the DEF pump, carefully remove compensator (3).


    Illustration 8g06278356
    (A) 38 mm (1.5 inch)
    (B) 97 mm (3.8 inch)

  6. Check the measurements of compensator (3). Check if the measurements are greater than specified in Illustration 8. This condition indicates that the DEF pump is contaminated with hydrocarbons.

  7. If the measurements indicate contamination, flush the DEF tank. Refer to Systems Operation, Testing and Adjusting, Diesel Exhaust Fluid Tank - Flush for the correct procedure.

  8. If the measurements are within the specification, continue to follow the appropriate troubleshooting procedure to determine if the DEF pump has a fault.

    Note: If there is no DEF contamination, proceed to "Test Procedure For DEF Concentration".

Test Procedure For DEF Concentration



    Illustration 9g03370564
    A typical example of Tooling (A)


    Illustration 10g03370553
    Calibration point for distilled water

  1. Follow the instructions included with Tooling (A) to calibrate the waterline of the meter.

  2. Clean Tooling (A) and apply two drops of Diesel Exhaust Fluid (DEF) collected from the DEF tank.


    Illustration 11g03370573
    Typical reading for DEF in good condition

  3. Inspect the DEF in Tooling (A). The DEF quality must measure between 29 and 35 percent. If the DEF does not meet specification, replace the DEF in the tank with new DEF. Refer to Operation and Maintenance Manual for more information. The new DEF must meet ISO 22241 standards.

    Note: Dispose of the DEF removed as per local regulations and mandates.

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